Pulse program: jcc.bv ---------------------------------------------------------------- ;2D difference 13C CT-HSQC ;for determination of J3(C'Cb) ;in Val, Ile, and Thr residues ;for the determination of X1 angle ;Grzesiek, S., Vuister, G.W., Bax, A. ;JBNMR 1993, 3, 487-493. ;Spectra are acquired as interleaved pairs of ;13C echo/antiecho pairs with 15N decoupled ;in first expt, and coupled in second expt ; ;Implemented and tested on DMX-600 by B. Volkman, ;volkman@nmrfam.wisc.edu. 7/4/96 BFV ;fixed phase problem in t1 1/7/96 BFV ; ;Updated and tested on NMRFAM DMX-600 by B. Volkman, ;volkman@nmrfam.wisc.edu 042200 ; added multiblock acquisition: wr#1 and wr#2 ; commands for each part of expt to allow processiong ; in Xwinnmr (and nmrPipe) without disentangling ; FIDs from coupled/decoupled expts. ---------------------------------------------------------------- Installation: 1. Copy the jcc.tar file to your experiment directory on the spectrometer (/u/data/username/nmr). 2. Unpack the tar file with 'tar -xvf jcc.tar'. 3. Place additional files in appropriate directories (e.g., grad program in gp dir, pulse program in pp dir, *.incl files in pp dir, etc). 4. Find jcc in your directory in XwinNMR (dir or browse), adjust pulse widths, offsets, frequencies as needed for your machine before running experiment. ---------------------------------------------------------------- Files included with this archive: Avance.incl Gradfa.incl README acqu acqu1 acqu1s acqu2 acqu2s acqus bvjcc cag_par cpdprg3 format.temp grdprog.r jcc.bv pdata/ pulseprogram scon spnam4 ----------------------------------------------------------------