Pulse program: jnc.bv ---------------------------------------------------------------- Description: ;jnc.bv ;2D difference 13C CT-HSQC ;for determination of J3(NC) ;in Val, Ile, and Thr residues ;for the determination of X1 angle ;Vuister, G.W., Wang, A.C., Bax, A. ;JACS 1993, 115, 5334-5335. ;Spectra are acquired as interleaved pairs of ;13C echo/antiecho pairs with 15N decoupled ;in first expt, and coupled in second expt ; ;Implemented and tested on DMX-600 by B. Volkman, ;volkman@nmrfam.wisc.edu. 6/13/96 BFV ; ;Updated and tested on NMRFAM DMX-600 by B. Volkman, ;volkman@nmrfam.wisc.edu 042200 ; added multiblock acquisition: wr#1 and wr#2 ; commands for each part of expt to allow processiong ; in Xwinnmr (and nmrPipe) without disentangling ; FIDs from coupled/decoupled expts. ---------------------------------------------------------------- Installation: 1. Copy the jnc.tar file to your experiment directory on the spectrometer (/u/data/username/nmr). 2. Unpack the tar file with 'tar -xvf jnc.tar'. 3. Place additional files in appropriate directories (e.g., grad program in gp dir, pulse program in pp dir, *.incl files in pp dir, etc). 4. Find jnc in your directory in XwinNMR (dir or browse), adjust pulse widths, offsets, frequencies as needed for your machine before running experiment. ---------------------------------------------------------------- Files included with this archive: Avance.incl Gradfa.incl README acqu acqu1 acqu1s acqu2 acqu2s acqus bvjnc cag_par cpdprg3 cpdprg4 format.temp grdprog.r jnc.bv pdata/ pulseprogram scon spnam4 ----------------------------------------------------------------